仪器分类
Liquid chromatography_液相色谱仪
Liquid chromatography_液相色谱仪
仪器编号
83182
SN序列号
L21806102271
生产厂家
SHIMADZU
型号
LC-20AR
制造国家
Japan
分类号
放置地点
SA BuildingSA534
购置日期
2022-11-01
入网日期
2024-05-29

主要规格及技术指标

1. Wide Range of Liquid Delivery Flow Rates, Covering Semi-Microanalysis to Semi-Preparative
The liquid delivery flow rate range is extensive, allowing for selections from 0.001 to 20.00 mL/min. Due to the adoption of a parallel dual-plunger reciprocating pump drive system, even at low flow rates, it can ensure low pulsation and stable flow.
2. Cyclic Preparative Function
By installing an optional set of circulation components and circulation valves, closed-loop cyclic preparative separation can be achieved. The optimized design of the pump head with a minimal volume can reduce column external diffusion effects and improve cycling efficiency.
3.UV Detector:
It incorporates a built-in low-pressure mercury lamp for wavelength calibration and correction. The calibration is performed automatically during startup, and manual correction can be conducted at any time. It features the capability of simultaneous dual-wavelength determination.
Light Source: Deuterium lamp.
Wavelength Range: 190 – 700 nm.
Wavelength Accuracy: ±1 nm
Wavelength Precision: ±0.1 nm
4.Baseline Noise: Less than ±0.25 × 10⁻⁵ AU (measured at 250 nm, with constant room temperature and isopropanol in the flow cell), complying with ASTM standards.
Drift: Less than 1 × 10⁻⁴ AU/h;
Measurement Range: 2.5 AU
1.送液流速范围大,涵盖半微量分析到半制备
送液流速范围大,可在0.001-20.00mL/min 的范围内选择。由于采用了的并联双柱塞循环泵驱动方式,即使是低流速时也能确保较低脉动和稳定的流量,流速精确度0.1%RSD, 准确度 1%;
2. 循环制备功能
通过安装一套选配的循环组件和循环阀,可实现闭合环路循环制备分离。经过优化设计的泵头容积极小,可减少柱外扩散效应并提高循环效率;
3. 紫外检测器:内置低压汞灯用于波长校准及校正。开机时校准,随时可以进行校正,具有双波长同时测定功能;光源:氘灯;波长范围:190—700nm,波长准确度:±1nm,波长精确度:±0.1nm
4.基线噪音:低于±0.25×10-5Au(250nm,室温恒定,池内异丙醇),符合ASTM标准;漂移:低于1 х 10-4AU/h;测量范围:2.5AU

主要功能及特色

主要用于药物、天然产物和有机合成等目标化合物及杂质的分离、分析与制备。通过自动对色谱峰进行切割、区分,能够对纯化后的化合物进行色谱分析检测,软件全自动控制,无需手动切换。同时,全在线捕集、浓缩、纯化和回收系统,能够有效去除流动相中的改性剂,提高产物纯度和回收率
It is primarily utilized for the separation, analysis, and preparation of target compounds and impurities in pharmaceuticals, natural products, organic synthesis, and other fields. By automatically slicing and distinguishing chromatographic peaks, it enables chromatographic analysis and detection of purified compounds. The entire process is fully software-controlled, eliminating the need for manual switching. Additionally, the integrated online system for trapping, concentrating, purifying, and recovering substances can effectively remove modifiers from the mobile phase, thereby enhancing product purity and recovery rates.

主要附件及配置

LC-20AR Solvent delivery unit 溶液传输单元
Autosampler SIL-10AP自动进样
SPD-20A UV-VIS Detector紫外检测器
FRC-10A Fraction Collector 馏分收集器

公告名称 公告内容 发布日期
独立使用* 辅助使用
校内收费标准(元/小时) 校外收费标准(元/小时) 校内收费标准(元/小时) 校外收费标准(元/小时)
 ¥20.00    ¥40.00  ¥60.00

* 对校外用户不开放独立使用